# # arev:/usr/local/unicat/unireq/beamreq/req00081.txt # UNICAT Member Beam Time Request #81 # created Wed Sep 29 14:13:45 CDT 1999 # collaboration: Yes days: 5 description: Several months ago, we completed the first APS experiment to study magnetism in K2ReBr6 using resonant x-ray techniques. We found clear evidence of magnetic scattering associated with the Re LIII and LII edges. We quickly searched for scattering at the LI edge and Br K edge and found no clear evidence of such scattering. However, the experiment was somewhat limited by the geometry used and the shape of the radiation shroud. The experiment should be able to be greatly enhanced by the use of an extended face geometry with a cleaved and polished surface. In the meantime, we have performed powder neutron measurements which have allowed us to understand the low temperature structure which differs substantially from the room temperature structure (there are a series of phase transitions which transform the system from cubic to monoclinic). This should allow us to better understand the low temperature domain structure which has been clearly seen with both neutrons and x-rays. With these improvements, we expect to improve on the results obtained previously and to possibly be able to observe magnetic resonant scattering associated with the Br K edge. equipment+required: displex experiment: Magnetic X-ray scattering study of K2ReBr6 hazards: name: Mark D. Lumsden nonmembers: Mark D. Lumsden / Stephen E. Nagler station: 33ID-D unacceptable+dates: None #QUERY_STRING: #REMOTE_HOST: lumsden.ssd.ornl.gov #REMOTE_ADDR: 128.219.37.91 #CONTENT_LENGTH: 1505 #HTTP_REFERER: http://www.uni.aps.anl.gov/unireq.htm #HTTP_USER_AGENT: Mozilla/4.7 [en] (X11; I; Linux 2.2.11 i686)