#
# arev:/usr/local/unicat/unireq/beamreq/req00104.txt
# UNICAT Member Beam Time Request  #104

# created Wed Mar 15 16:51:41 CST 2000
#

collaboration:
	Yes

collaborator+Paul:
	on

collaborator+Pete:
	on

days:
	5

description:
	The major goal of this experiment will be to maximize the potential
	 of the synchrotron to aid in materials characterization by
	 collecting x-ray diffraction, x-ray fluorescence and x-ray near
	 edge absorption spectroscopy data from the same spot on the same
	 sample with the same experimental set up. Specifically we plan to
	 use an area detector to collect powder diffraction patterns of
	 unknown oxides (even mixtures of oxides), with data of sufficient
	 quality to use for phase identification, and in as short a time
	 period as possible. We will also explore the possibility of 
	simultaneously collecting XRF information to determine chemical
	 composition in at least a semi-quantitative manner. The third 
	part of the experiment will involve collecting XANES data on those
	 elements of interest, with the aim of determining oxidation state
	 information.
	The collaborators in the experiment will be Simon Bare, Bob Broach
	 and Rich Willis from UOP, and Gene Ice and Ki-Sup Chung from ORNL.
	

equipment+required:
	XYZ stage and Huber diffractometer
	Ion chambers, Huber slits, etc.
	ORNL will be supplying area detector and solid state fluorescence
	detector. 

experiment:
	Combined XRD, XRF %26 XANES studies of novel oxides

hazards:
	There are no specific hazards associated with this experiment.
	The samples are non-hazardous metals or metal oxides, and the
	data will be recorded at room temperature in air.

name:
	Simon R. Bare

new+request:
	on

nonmembers:
	None

station:
	33ID-D

unacceptable+dates:
	19-30 May; 23 June - 5 July
	
	Preferred dates: June 7-11



#QUERY_STRING: 
#REMOTE_HOST: lsx18bu.nsls.bnl.gov
#REMOTE_ADDR: 130.199.192.217
#CONTENT_LENGTH: 1766
#HTTP_REFERER: http://www.uni.aps.anl.gov/unireq.htm
#HTTP_USER_AGENT: Mozilla/4.5 [en] (Win95; I)