#################################################### # Eric D. Isaacs # requesting 5 days, at minimum=3 days # beamline 33BM, "Search for Charge ordering in Untwinned LSCO" #################################################### # top:/home/www/beamtime-requests/req00360.txt # UNICAT Member Beam Time Request #360 # created Mon Jan 13 09:09:53 CST 2003 #################################################### beamline: 33BM collaboration: Yes collaborator+Paul: on contact: isaacs@Lucent.com days: 5 description: The competition between the insulating states and superconductivity is a key feature of the high-TC problem, yet the character of the insulating state remains elusive. Striped density waves are one of the primary candidates for the insulating ground state. However, direct and unambiguous x-ray observation of any charge ordered state in the cuprates remains an outstanding problem in the high-TC community. In the past year, quasi-elastic Raman scattering data published in Science has provided some of the most compelling evidence for a pinned density wave in the quasi one-dimensional ladder compound Sr14Cu24O41. Very recently, unpublished results have shown a similar fingerprint of pinned charge density waves in the world's first untwined crystals of La2-xSrxCuO4. The keys to this finding, were the very low doping (x~0.01) and the fact that these samples were untwined. This past December we began the search for charge ordering in LSCO with 1% Sr at 20 K at 33BM. Measurements made in the [hk0]-plane, and just above and below this plane with delL=+/-0.1, showed evidence for two sets of two-fold peaks. The rectangular pattern indicates an anisotropic ordering of the doped holes. We propose making a similar set of x-ray measurements in an untwinned sample with 3% Sr. This will allow us to observe systematic variations in the pattern which would be important confirmaiton of the charge ordered state. A particular challenge is seperating out the scattering from the holes at very incommesurate positions and that due to the tails of the very bright (2,4,0) Bragg peak. We also plan to reorient the new samples with a* perpendicular to the surface. This will ensure that our highest resolution will be along the direction of the largest incommensurability as observed in measurements from the Fall. equipment+required: displex w/Be dome experiment: Search for Charge ordering in Untwinned LSCO foreign+nationals: Yoichi Ando, CRIEPI, Tokyo hazards: none minimumdays: 3 name: Eric D. Isaacs nonmembers: Eric D. Isaacs, Bell Labs Girsh Blumberg, Bell Labs unacceptable+dates: #REMOTE_HOST: Host 14.20.104.135.in-addr.arpa not found: 3(NXDOMAIN) #REMOTE_ADDR: 135.104.20.14 #CONTENT_LENGTH: 2414 #HTTP_REFERER: http://www.uni.aps.anl.gov/unireq.htm #HTTP_USER_AGENT: Mozilla/4.76 [en] (Windows NT 5.0; U)