#################################################### # Andrew Allen # requesting 3 days, at minimum=2 days # beamline 33ID, Temperature-Mediated Nanoparticle Nucleation and Growth # instrument 33ID-D USAXS #################################################### # top:/home/www/beamtime-requests/req00690.txt # UNICAT Member Beam Time Request #690 # created Fri Dec 03 15:13:21 CST 2004 #################################################### apsrun: 2005-01 beamline: 33ID collaboration: Yes collaborator_Pete: ON contact: andrew.allen@nist.gov days: 3 description: Following some modifications to the NIST USAXS Fluid Flow Cell, we request a 2-day experiment to study temperature-dependent solution-mediated nucleation and growth of copper oxide and cerium oxide nanoparticulate dispersions. This will require temperature control of the flow cell, which was not possible in the recent run due to problems with the USAXS instrument that affected 3 of the 5 days allocated. equipment_required: Regular USAXS instrument at 10-11 keV energy. experiment: Temperature-Mediated Nanoparticle Nucleation and Growth foreign_nationals: hazards: Some handling of aqueous surfactants, acid, base, possibly toluene. Normal lab precautions will be taken. We wil run air extractor fan in hutch if running toluene. instrument: 33ID-D USAXS instrument_other: minimumdays: 2 name: Andrew Allen nonmembers: unacceptable_dates: Please do NOT schedule before March 1st, 2005. April 10-13, 2005 (American Ceramic Society meeting). z34ID_details: #REMOTE_HOST: porcelain.nist.gov #REMOTE_ADDR: 129.6.180.24 #CONTENT_LENGTH: 1099 #HTTP_REFERER: http://www.uni.aps.anl.gov/unireq.htm #HTTP_USER_AGENT: Mozilla/5.0 (Macintosh; U; PPC Mac OS X; en) AppleWebKit/125.5.5 (KHTML, like Gecko) Safari/125.11