#################################################### # Joo Kang # requesting 5 days, at minimum=4 days # beamline 33BM, XAFS study of supported Pt clusters # instrument 33BM-B XAFS #################################################### # top:/home/www/beamtime-requests/req00921.txt # UNICAT Member Beam Time Request #921 # created Mon Jan 09 12:26:03 CST 2006 #################################################### apsrun: 2006-01 beamline: 33BM collaboration: No collaborator_Jenia: ON contact: kang@mrl.uiuc.edu days: 5 description: Structural and electronic properties of supported Pt clusters will be investigated in relation to the cluster-support interaction. From the last experiment, we found that the strong interaction between support and cluster has significant impact on the nature of the metallic clusters after the cluster has been reduced. To further investigate this effect both the clusters and support will be measured with XAFS at different temperature ranges (150 K to 600 K). Pt clusters supported on different oxide support (alumina) will be studied to understand the effect of the support structure to the effect of the metallic clusters. equipment_required: experiment: XAFS study of supported Pt clusters foreign_nationals: Joo Kang hazards: Materials to be used: Liquid nitrogen to control sample temperature Heating element to control sample temperatures to 600 K max. 1% H2 in He balance 10 % O2 in He balance instrument: 33BM-B XAFS instrument_other: minimumdays: 4 name: Joo Kang nonmembers: submit: Submit unacceptable_dates: Note. If possible I'd like to have at least several days apart from the beamtime submitted by Laurent Menard. We will participate on both of our proposed experiments and we found it would be better to have at least a few days between the two beamtime. Thanks. z34ID_details: #REMOTE_HOST: nuzzopc16.mrl.uiuc.edu #REMOTE_ADDR: 130.126.102.167 #CONTENT_LENGTH: 1432 #HTTP_REFERER: http://www.uni.aps.anl.gov/admin/unireq.html #HTTP_USER_AGENT: Mozilla/4.0 (compatible; MSIE 6.0; Windows NT 5.1; SV1; .NET CLR 1.1.4322)