#################################################### # Ruqing Xu # requesting 6 days, at minimum=6 days # beamline 33BM, TDS temperature dependence study # instrument 33BM-C fourc #################################################### # top:/home/www/beamtime-requests/req01042.txt # UNICAT Member Beam Time Request #1042 # created Fri Aug 25 17:51:28 CDT 2006 #################################################### apsrun: 2006-03 beamline: 33BM collaboration: Yes contact: ruqingxu@uiuc.edu days: 6 description: We are continuing our study of TDS temperature dependence with line scans. In the July 2006 run, the data for T-branch scans have yielded good quantitative result of phonon frequencies, which proves that our approach is plausible; however, we still need to improve our signal-noise ratio for the L-branch phonons, as well as longer time to study more k-points in the reciprocal space to make a complete story. We will also revise the sample holder to ensure a clean signal. Basic description: X-ray incident on a single crystal sample of Cu(or Nb), which will be mounted in a displex with a heater to control its temperature. TDS intensity will be measured with a point detector at different k-points and different temperatures. We are considering the choice between 33BM-C and 33ID-D; the latter has the advantage of a brighter beam and thus faster data-collection rate. But if the goneometer in ID-D is not ok for this task, then a relatively longer beamtime in BM is needed. equipment_required: displex, vaccuum pump, temprature controller experiment: TDS temperature dependence study foreign_nationals: Ruqing Xu, Hawoong Hong, Jaseung Ku hazards: Cu sample might need to be processed with nitric acid, wich is corrosive & toxic. instrument: 33BM-C fourc instrument_other: minimumdays: 6 name: Ruqing Xu nonmembers: Hawoong Hong, Jaseung Ku submit: Submit unacceptable_dates: z34ID_details: #REMOTE_HOST: chiangpc12.mrl.uiuc.edu #REMOTE_ADDR: 130.126.102.112 #CONTENT_LENGTH: 1534 #HTTP_REFERER: http://www.uni.aps.anl.gov/admin/unireq.html #HTTP_USER_AGENT: Mozilla/4.0 (compatible; MSIE 6.0; Windows NT 5.1; SV1; .NET CLR 1.1.4322)